Process NMR Associates LLC

Home

About Us

NMR Service

Pricing

Service Request

SubmissionForm

Liquids Apps

Solids Apps

Process NMR

Process Apps

Spin Track

RefinIR

Lab NMR

NMR Blog

Experience

Services

Facilities

Directions

NMR Overview

Chemometrics

Training

Reference

Manuals

FAQ

Links

Blog Methods

Blog Summary

Contact:

John Edwards

(203) 744-5905

 

Applications - Capabilities of NMR

NMR Based Analyses that Have Been Recently Performed by Process NMR Associates

Crude Oil Analysis - TBP and Other Assay Information, Average Molecule Parameters, Hydrogen Content

Hydrocarbon Fuel Analysis - Diesel, Kerosene, Gasoline, Cycle Oils, Biomass Conversion Products

Cracked Petroleum Product Analysis - Olefin Speciation in Naphtha, ICCS, HCCS, Coker Naphtha, Coker Gas Oils

Olefin Analysis of Cracked Products by NMR

Expert Witness and Court Case Related Technical Services 

Lubricant Oil - Detailed Chemistry Analysis by 13C NMR

Training of Petroleum Company NMR Personnel in Detailed Hydrocarbon Analysis by Liquid and Solid-State NMR

Training of Petroleum Company NMR Personnel in Chemometric Applications in NMR of Petroleum Products

31P NMR Analysis of Zinc and Molybdenum Thiophosphate and Thiocarbamate Anti-Wear Additives

Chemometric Analysis Correlating NMR of Petroleum and Petrochemical Products with Chemical and Physical Properties

Heavy Petroleum Characterization - Heavy Oils, Residues, Vacuum Gas Oils, Shale, Kerogen, Tar Sands, Bitumen, Tar, Pitch

Asphaltene Analysis by Liquid and Solid-State 1H/13C NMR

Edible Oil Analysis - 1H, 13C and 31P NMR of Oils - Stability Studies, Classification Studies, Adulteration Detection

Essential Oils Analysis - 1H and 13C NMR - Identification and Adulteration Detection

Product Purity Analysis - USP <761>

Aloe Vera Quality Analysis - 1H NMR Method for Quality Inspection, Identification and Adulteration Detection - see details.

Nopal Quality Analysis - Method Developed Similar to IASC Aloe Vera Test

Quantitative Analysis and Authentification of Gum Arabic and Other Commercial Gums by 13C and 1H NMR

Competitive Analysis - Polymers, Commercial Additive Products

Automobile Fuel Tank Contaminant Analysis

Troubleshooting NMR Analysis of Problematic Materials (Deposits, Sludge, Process Fouling Materials).

Engine Deposit Analysis by Solid-State 13C NMR - Combustion Chamber Deposits (CCD), Intake Valve Deposits (IVD), Crankcase Sludge

Correlation of Fuel Chemistry with Deposit Fromation Tendancies - Effects and Quantification of Additives

2H NMR Tracer Studies of D2O and Other Deuterated Molecules in Fuels and Reaction Processes  

Solid-State 13C NMR of Diesel Engine Soot 

Naphtha Analysis - Full Speciated PIONA by NMR

FCC and RCC Feed Analysis by 13C NMR - Carbon PNA Values + Average Molecule Description for Reactor Model Development.

Catalyst Characterization - Solid-State NMR - 27Al, 31P, 29Si of Molecular Sieves and Heterogeneous  Catalysts

Catalysts Deactivation Studies - 13C and 29Si Coking

Service and Development of Predictive Models Utilized in 30+ Online NMR Systems Engaged in Process Control and Optimization

Polymer Additive Identification 

Small Molecule Characterization - (1D, 2D (COSY, NOESY, HETCOR, HMBC, HNQC), and Multinuclear NMR)

Mobile NMR Projects with Low Field Spectrometer and Surface Explorer Probe/Magnet - Literally NMR in your Hands.

Lipids Analysis

NMR Laboratory Instruction at Marist College

Instruction and Mentoring of Undergraduates Engaged in Multi-Year Analytical Research Projects

Instruction and Technical Support of Academic NMR Facilities

Lignocellulosics and Cellulose Analysis Related to Biorefinery Applications

Ethanol Fuel Analysis by 1H and 13C NMR

Lycopene Analysis from Extractive Process

Alkene Analysis by 1H and 13C NMR

Polymer Analysis - Detailed Backbone Analysis - Many Kinds of Polymers - Nylons, Acrylates, Acrylics, Polyesters, Polyimides, etc.

Polymer End-Group Analysis and Molecular Weight Calculation by NMR - Nylons, Acrylates, Acrylics, Polyesters, Polyimides, etc.

Tagging Experiments - Identification of Labile Hydrogen Functionality by Reaction With Chlorophospholane and 31P NMR

119Sn Tagging NMR - Mercaptan, Alcohol, Phenol, Acid, Amine Characterization 

Solid-State NMR of Gasification and Pyrolysis Feed Streams - Slurries, Plastics, Sewage, Cellulosics

Black Liquor Analysis by 13C and 1H NMR

Red Oil and Acid Strength Analysis of Acid Alkylation Sulfuric Acid by 1H NMR

USP and ASTM (D4273-05 / D4875-05) Poloxamer Analysis by 1H and 13C NMR

Butyl-Tin Quality Analysis by 119Sn NMR

77Se NMR 

Animal Fats - Biodiesel Conversion Process and Products Analysis

Liquid- and Solid-State 13C NMR of Collagen

EPDM, EPDM-PP, Ethylene Propylene, Ethylene-Propylene-Butylene Terpolymer Analysis by 13C and 1H NMR

Phosphorus Chemistry Analysis by 31P NMR

Relaxation Measurements (T1, T2, TCH, T1r) at Low and High Field

Coal Analysis by Solid-State 13C NMR

Solid-State NMR of Tobacco

Solid-State NMR Analysis of Herbs and Spices - Authentification

Process Analysis by Online NMR - Refinery and Petrochemical Applications (See Process NMR Applications)

Heavy Water (D2O) Purity Analysis

Polyvinyl Alcohol Analysis by Solid-State NMR and Low Resolution TD-NMR - wwelling and crosslinking studies.

Contrast Agent Analysis by 13C or Relaxation Analysis

Gasket and Rubber Analysis by Multinuclear (1H,13C,29Si NMR and Relaxation (T1,T2)Analysis 

NMR of Adhesives - 1H-13C-29Si

Rubber Analysis by Low Field NMR Surface Probe - Curing and Cross-Linking by 1H Echo and CPMG Experiments

Cement Analysis - Solid-State 1H, 29Si, 27Al NMR - Relaxation Studies

Moisture Content of Cement and Many Other Materials by Low Field NMR

Lignin Characterization - Solid-State 13C NMR

Sodium Analysis of Food and Beverage by 23Na NMR

Carbohydrate and Polysaccharide Analysis - Liquid and Solid-State 1H, 13C and 17O NMR

Process Fluids Analysis - Chip Manufacturing 

Surface Modification of Medical Device Materials - Solid-State 19F, 29Si, 13C NMR

Structure - Activity Determination and Correlation (Polymers, Additives, Petroleum Products)

Dairy Product Analysis by NMR - Cheese, Milk, Cream Cheese, Evaporative Process Intermediates

Contamination Analysis 

Time-Domain NMR Analysis of Soap - Physical Property Relationships to T2 and T1 Relaxation

Humic Acid and Fulvic Acid Analysis by Liquid and Solid-State NMR

NMR Relaxometry of Cheese

Moisture Analysis by Low Field NMR

Inverse Laplace Transformations Yielding T2 Distributions

Spin Finish of Fibers by Low Field NMR

Solid Fat Content by Low Field NMR

Total Hydrogen Content by Low Field Pulsed NMR (ASTM D7171-05 / D3701-01 / D4808-01)

Aromatic Carbon Contents of Hydrocarbon Oils by High Resolution Nuclear Magnetic Resonance Spectroscopy (D5

Determination of Linear Low Density Polyethylene (LLDPE) Composition by Carbon-13 Nuclear Magnetic Resonance (D5017-96)

31P, 23Na and 1H NMR of Cheese

13C Solid State NMR Analysis of Food Adulteration - Particularly Gums and Maltodextrin Adulteration

Liquid-State NMR Analysis of Food Adulteration

Adulteration of Gum Arabic - by Liquid and Solid-State 13C NMR 

17O NMR Analysis of Water

1H/13C/31P NMR of Oligonucleotides

Adulteration of Licorice with Maltodextrin by Liquid and Solid-State 1H/13C NMR

Trans- Fat Analysis in Oils by 1H and 13C NMR

Biodiesel Analysis by 1H and 13C NMR - Transesterification Process Monitoring and B20 and B100 Quality Measurement

Biomass Analysis - 13C NMR

Gas-to-Liquids Product Analysis - Detailed iso-paraffin analysis by 13C NMR required for patent infringement issues.

Filter Contamination Assessment - 13C NMR of Dirty and Clean Filters for Identification of Causes of Low Flow.

Biomass-to-Fuels Conversion - Solid-State 13C NMR

Waste-to-Liquids, Coal-to-Liquids, and Gas-to Liquids Liquid Product Analysis by FT-IR, NMR, and Simulated Distillation

Dimethyl Ether (DME) Product Analysis by NMR

Development of Low Cost NMR Consoles to Upgrade RF Electronics in Benchtop NMR Systems

Dairy Product Analysis - Fat Content, Water Content - by Low-Field NMR

Polymer Cross-Linking Studies Utilizing Variable Contact Time Experiments

Amorphous Content of Pharmaceutical Solids

Polymorph Identification by Solid-State 13C NMR

Pesticide Phosphorus Chemistry by 31P NMR

Fischer-Tropsch Hydrocarbon Product Analysis by 1H and 13C NMR - Detailed iso-paraffin analysis by 13C NMR 

Application of Detailed NMR Analysis to Intellectual Property Issues

Olefin Analysis of Synthetic Fuels

Development of Low Cost NMR Consoles to Upgrade RF Electronics in Superconducting NMR Systems

Chemometric Regression Development Chemical and Physical Properties of Synthetic Fuel 

Polyurethane Reverse Engineering 

Development of Benchtop Permanent Magnet NMR Systems

Development of Low Cost Superconducting NMR System Spectrometer

Specialty Coating Formulation Analysis by NMR

Polyurethane Prepolymer Formulation Analysis by NMR

Quantitative Acrylate Polymer Analysis of Complex Mixtures by 1H and 13C NMR

Caprolactone, Adipate, Neopentyl Glycol, Hexandiol, Butandiol, Ethylene Glycol, Methacrylate, BuMA, MMA Component Mixtures

Termination Chemistry Probes by 31P NMR of Chlorophosphalane Derivatives

Adhesives Chemistry Analysis by NMR

Inclusion Complex Analysis - Variable Contact Time Experiments

2H Food Authentification Methodologies

Oil/Water Emulsion Characterization 

Teflon and ETFE Studies Utiling 1H-13C and 19F-13C Solid-State NMR Analysis

Multinuclear NMR (1H, 31P, 23Na) Analysis of Salt Formation in Cheese

Oil-Fat-Water Analysis of Food Stuffs by High Field and Low Field NMR

Natural Product NMR Analysis

Wind Turbine Oil Analysis by 31P and 1H/13C NMR

Polyol and Polyether Analysis by NMR - 1H and 13

Functionalized Polyolefin Analysis by Liquid and Solid-State NMR

Solid-State 13C NMR of Extraterrestrial Material - Meteors and Comets

Solid-State 13C NMR of Materials Created During Cometary Impacts

Biotechnology Small Molecule Analysis by 1H NMR

Bulletproof Vest Analysis by Solid-State 31P and 13C NMR Analysis

Solid-State NMR of Polyvinyl Alcohol and Other Gel Materials

Solid-State 13C NMR Analysis of Nanodiamonds, Nanocarbon, Activated Carbons and Charcoals

Solid-State and Liquid-State NMR of Modified Fullerenes

1H and 13C NMR of Extracted Soils from Oil Spill Locations for Crude/Petroleum Product Identification

European Pharmacopoeia - Fish Oil Analysis - 13C NMR of Fatty Acid Distribution

Oil in Seeds by Low Field NMR 

1H and 13C NMR Analysis of Acacia senegal, Acacia seyal, Acacia polyacantha, Combretum

Spin Diffusion (DOSY) NMR Analysis

GC analysis of Essential Oils

Analysis and Comparison of Flame-Retardent Polymers 

1H and 13C NMR of Inclusion Complexes in Cyclodextrins

1H and 13C NMR of BASF Pluronics®

Solid-State and Low Field NMR of Clays

Polynuclear Aromatic Distributions in Petroleum by 1H NMR Analysis - Correlation to UV and HPLC/UV Methods

Simulated Distillation Analysis of Crude Oils - Relationships to 1H and 13C NMR 

Simulated Distillation Analysis of VGO and Slurry Oils - Relationships to 1H and 13C NMR

Simulated Distillation Analysis of Diesel Fuels - Relationship to NMR and Sulfur Analysis

GC Simulated Distillation Analysis - D2887, D3710, D5307, D6352

Transformer Oil Analysis

Hydrogen Content Analysis and Method Development in Middle Distillates and Heavy Petroleum Residues by ASTM D-7171

Cyclodextrin-Vitamin E and PEO-Thiourea Inclusion Complexes by Solid-State NMR

UHMWPE - Solid-State 13C NMR Analysis

Inverse Laplace Transformation of CPMG Profiles Obtained from Food, Cosmetic, and Petroleum Products

Solid Fat Content Analysis of Shea Butter, Chocolate, Dairy Butter by TD-NMR

Chitosan Acetylation Determination

FTIR-ATR - Chemometric Model Development for FCC/RCC Feed and Diesel Analysis. 

Development of 1H NMR Methodologies to Calculate Detailed 13C NMR Structural Parameters in Petroleum Products and Crude Oils

Development of Magnetic Field Independent NMR Multivariate Statistical Models to Predict Chemical and Physical Properties of Petroleum

1H and 13C NMR Analysis of Polar and Apolar Fractions in Butter and Margarine

Process NMR Application for Butter Analysis - Oil/Fat Ratio

Construction of 60 MHz TD-NMR Magnet and Spectrometer

Development of TD-NMR Spectrometer Console for Upgrading Older Minispec and Oxford Instrument Machines

Unilateral NMR Analyzer Development

Coal and Petroleum Asphaltene Analysis by Liquids and Solids 13C and 1H NMR

In-Situ Combustion and Catalysis Products Analysis

Fischer Trospch CTL and GTL Products Analysis - Diesel and Jet Fuel

Correlation of PAH Distributions to 13C and 1H NMR Analysis

Raman, FTIR-ATR, NMR, SimDis - Combined analysis of Diesel Fuels

ESR Analysis of Vanadium and Organic Radicals in Crude oils, Residues, and Cracker Feeds.

Combination of NMR and ESR in a Single Platform Analyzer

Sodium Analysis of Snack Foods and Soups by Low Field NMR Instrumentation

Nanomaterials Analysis by Multinuclear NMR Spectroscopy and Relaxation Comparisons 

Correlation of Diesel Carbon Number Distributions - Simulated Distillation Analysis Correlated to NMR

FTIR-ATR Database Development for Petroleum Products, Essential and Edible Oils, Polyurethane

 

 

For more information on this topic please contact:

John Edwards

Manager, Process and Analytical NMR Services

Process NMR Associates LLC,

87A Sand Pit Rd

Danbury, CT 06810, USA

Tel: (203) 744-5905