Process NMR

Process NMR Associates - Pricing Schedule                                          Effective 2012

Standard Rates are Charged for Spectrometer Time and Professional Time

We will Competitively Discount any Quote Obtained from a Commercial NMR Service !!!
Typical Turnaround Time: 1-3 Days from Receipt of Samples. Same Day Priority Turnaround Available on Demand *

Sample Submission - Follow this link for details on how to submit a sample.

 

NMR Spectrometer Time
(includes spectrometer set up and routine sample prep).

  • Standard Rate : $80/hr (For First 4 hours), $35/hr for additional hours over 4 hours (Overnight $450, 24 Hour Acquisitions $750).
  • Priority Service*: $160/hr for immediate priority. Charge based directly on time to prepare samples, perform analysis and report.
  • Process FT-NMR and Time-Domain Relaxometer Investigations: $80/hr
  • Time-Domain NMR Tests - Charged on a per test basis - call for quote.
  • Professional Time for Interpretation and Non-Standard NMR Related Services: $175 /hr.
* Subject to availability - please inquire

NMR - Individual Experiments:

  • Standard 1H Analysis : $50 ** (No analysis/interpretation of data/assuming sample not limited (>2 mg))
  • Standard 13C Analysis : $250 ** (No analysis/interpretation of data/assuming sample is not limited (>300 mg))
  • Quantitative 13C NMR : $350-450 ** (High S/N acquired).
  • Detailed 13C Analysis with average molecule parameters calculated: $450**
  • Standard 1H-13C DEPT : $80** (No analysis/interpretation of data)
  • Multidimensional experiments charged for actual spectrometer time. Overnight Acquisitions - $450  24 Hour Acquisitions $750).
  • ASTM F2259 Alginate Analysis - $225 ** (Assumes Sample Preparation Performed by Customer)
  • ASTM D7171 - Hydrogen Content of Middle Distillate Fuels by Pulsed NMR - $100 set up fee, $50 per sample
  • Aloe Vera Analysis - $135 (> 5X), $225 (<5X, includes freeze drying) **
  • Multinuclear and sample-limited experiments will be performed for a length of time that is agreed upon in advance.
  • NMR Identity Testing for REACH Registration - Call for Quote
  • NMR Tests Performed - Call for Quote
 ** Includes NMR Tube and Standard Deuterated Solvents !!
See Additional Charges that May be Levied Depending on Project Listed Below.

Consulting and Interpretation Fees:

  • Consulting fees are charged at a rate of $175/hr or $1200/day, plus usual/customary expenses.
  • (Initial discussions concerning a potential project are not considered consulting time).
  • Expert Witness $350/hr.
  • Professional Time Associated with NMR Technical Support of Litigation $250/hr

Low Resolution (TD) NMR Service:

  • T2, CPMG, Inverse Laplace Transformations, T2 Distributions, T1, T1 Distributions - $60 per sample
  • ASTM D7171 - $50 (all batches of samples will be charged a $100 set-up and calibration fee).
  • Temperature Profiles - $150 Per Sample

Simulated Distillation:

  • D2887 - Boiling Range Distribution of Petroleum Fractions by Gas Chromatography - $200 per Sample
  • D3710 - Boiling Range Distribution of Gasoline and Gasoline Fractions by Gas Chromatography - $275 per Sample
  • D5307 - Boiling Point Distribution of Crude Oil by Gas Chromatography - $275 per Sample
  • D6352 - Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography - $275 per Sample

Other Analytical Techniques - GC, GC-MS, FT-IR

  • Call for dedicated quote.

!! Additional charges:

  • Non-Standard Solvents - customer will be charged at cost for solvents other than CDCl3, DMSO-D6, or D2O.
  • Sample Tubes - Customer will be charged at cost for non-standard NMR tubes.
  • Sample Disposal - Customer will be charged at cost for this service. Typically $5 per sample for disposal.
  • Sample Return involves transportation to, and shipment by, a Certified HazMat Shipping Company - cost charged to customer.
  • Report Mailing - Customer will be charged at cost for expense of mailing reports by next-day mailing service.
  • Sample Pick-Up - Samples can be picked up within a 30 mile radius of Danbury at a rate of $40/hr driving time**

Process NMR Application Development

Process NMR Acquisition and Chemometric Modeling of Process Stream Sample Sets Available at Rates Negotiated Under an Application Development Agreement (Petrochemical, Refining, Food, Pharmaceutical Applications).

Liquid-State NMR Experiments    2 x Varian Mercury-300 Spectrometers

  • Varian 5mm 4-Nucleus Probe (1H/13C/19F/31P-2H)
  • Varian 5mm Broad Band Probe with PFG (1H-X-2H)
  • Varian 10mm Broad Band Probe (1H-X-2H)
  • Nalorac 20 mm Broad Band Probe (1H-X-2H)
  • Standard Acquisition, 1H-1H COSY, 1H-13C DEPT, 1H-13C HETCOR, Relaxation Studies, Multinuclear (27Al, 17O, 11B, 19F, 31P, 23Na, 2H, 29Si etc)

Solid or Liquid-State NMR Experiments    Varian UnityPlus-200 Spectrometer

  • Doty Scientific Multinuclear 7mm Supersonic Magic Angle Spinning Solids Probe (13C, 27Al, 11B, 19F, 31P, 23Na, 2H, 29Si etc)
  • Varian 5mm Broad Band Liquids Probe (1H-X-2H)
  • Single Pulse Acquisition, Cross Polarization (Variable Amplitude), CP Relaxation Studies, T1/T2 Relaxation Studies

Process NMR Analysis (At-Line, Batch, and On-Line)
Process NMR Spectrometers (3)

  • Qualion 57.8 MHz High-resolution "C-Type" Process FT-NMR (1H NMR)
  • Qualion 58.3 MHz High-resolution "D-Type" Process FT-NMR with ambient-100oC Variable Temperature Capability
  • Aspect Italia 60.2 MHz High-resolution NMR
  • Multivariate Analysis of Spectral Databases (NMR, NIR, and FTIR) - Eignevector Research Solo 6.5 and PLS-Toolbox for Matlab
  • Multivariate Analysis of Spectral Databases - Infometrix Pirouette and Thermo Grams AI with PLS/IQ

Time-Domain NMR Analysis (H-Content, SFC Analysis, Oil in Seeds, Oil in Water, Moisture Analysis)    

  • SpinTrack NMR Low Resolution NMR - Multinuclear (1H, 19F, 11B, 23Na, 31P, 27Al) 10 mm Probes, 1H Surface Probes. Standard Methods Performed.
  • Cosa Xentaur Spin Pulse TD-NMR - 10, 20, and 40 mm sample size magnet/probe systems - interchangeable spectrometer

Gas Chromatography - Simulated Distillation

  • Shimadzu GC-2010 - Simulated Distillation Analyzer

Gas Chromatography - Mass Spectrometry

  • HP 5890 A with HP 5970 Mass Selective Detector
  • HP 5890 A with FID Detector

Mid-FTIR-ATR  
  • Smiths Detection IdentifyIR ATR - Mid-Infrared Spectroscopy on Solid or Liquid Samples

Other Analytical Equipment

  • Karl-Fisher Moisture Analyzer
  • Convection Oven
  • 0.1 mg Balance
  • Micro-ESR Spectrometer
  • UV-Vis Spectrometer
  • Petrometrix NIR Spectrometer
  • Virtis Benchtop Freeze Dryer
  • pH Meters/Centrifuge
 Sample Submission - Follow this link for details on how to submit a sample.

Contact John Edwards for Quotes or Discussion Tel: +1 (203) 744-5905

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