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Contact:
John
Edwards
(203) 744-5905
| |
Rates
- Standard
Rates are Charged for Spectrometer Time and Professional Time
We
will Competitively Discount any Quote Obtained from a Commercial NMR Service
!!!
Typical
Turnaround Time: 1-3 Days from Receipt of Samples. Same Day Priority
Turnaround Available on Demand *
NMR Spectrometer
Time - 1 Hour Minimum (includes spectrometer set up and routine sample prep).
 | Standard Rate :
$80/hr (For First 4 hours), $35/hr for additional hours over 4 hours
(Overnight $500, 24 Hour Acquisitions $800). |
 | Priority Service*: $160/hr for immediate priority. Charge based directly on time to prepare
samples, perform analysis and report. |
 | Process FT-NMR and
Time-Domain Relaxometer Investigations: $80/hr |
 | Time-Domain NMR
Tests - Charged on a per test basis - call for quote. |
 | Professional Time
for Interpretation and Non-Standard NMR Related Services: $175 /hr. |
* Subject
to availability - please inquire
NMR - Individual
Experiments:
 | Standard 1H
Analysis : $45 each** (1 hour minimum, no
analysis/interpretation of data/assuming sample not limited (>10
mg)) |
 | Standard 13C
Analysis : $240** (No analysis/interpretation of data/assuming sample is
not limited (>500 mg)) |
 | Detailed 13C
Analysis with average
molecule parameters calculated: $350** |
 | Standard 1H-13C
DEPT : $80** (No analysis/interpretation of data) |
 | Multidimensional
experiments will be charged for actual spectrometer time. (Overnight
Acquisitions - $500, 24
Hour Acquisitions $800). |
 | Multinuclear and
sample-limited experiments will be performed for a length of time that is agreed
upon
in advance. |
** Includes NMR Tube
and Standard Deuterated Solvents !! See Additional Charges that May be
Levied Depending on Project Listed Below
Consulting and
Interpretation Fees:
 | Consulting fees are
charged at a rate of $175/hr or $1200/day, plus usual/customary expenses. |
 | (Initial discussions
concerning a
potential project are not considered consulting time). |
 | Expert Witness $350/hr. |
 | Professional Time
Associated with NMR Technical Support of Litigation $250/hr |
Low Resolution
(TD) NMR Service:
 | T2, CPMG, Inverse
Laplace Transformations, T2 Distributions, T1, T1 Distributions - $60 per
sample |
 | Temperature Profiles
- $150 Per Sample |
Simulated
Distillation:
 | D2887 - Boiling
Range Distribution of Petroleum Fractions by Gas Chromatography
- $200 per Sample |
 | D3710 - Boiling
Range Distribution of Gasoline and Gasoline Fractions by Gas
Chromatography - $275 per Sample |
 | D5307 - Boiling
Point Distribution of Crude Oil by Gas Chromatography - $275 per Sample |
 | D6352 - Boiling
Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C
by Gas Chromatography - $275 per Sample |
Other
Analytical Techniques - GC, GC-MS, FT-IR
 | Call for dedicated quote. |
!! Additional
charges:
 | Non-Standard
Solvents - customer will be charged at cost for solvents other than CDCl3,
DMSO-D6, or D2O. |
 | Sample Tubes -
Customer will be charged at cost for non-standard NMR tubes. |
 |
Sample Disposal - Customer will be charged at cost for this service.
Typically $5 per sample for disposal. |
 | Sample Return
involves transportation to, and shipment by, a Certified HazMat Shipping
Company - cost charged to customer. |
 | Report Mailing
- Customer will be charged at cost for expense of mailing reports by
next-day mailing service. |
 | Sample Pick-Up - Samples can be picked up within a 30 mile radius of Danbury at a rate of
$40/hr driving time** |
Process
NMR Application Development
Process
NMR Acquisition and Chemometric Modeling of Process Stream Sample Sets
Available at Rates Negotiated Under an Application Development Agreement
(Petrochemical, Refining, Food, Pharmaceutical Applications).
Liquid-State
NMR Experiments Varian
Unity-300 Spectrometer
 | Varian
5mm 4-Nucleus Probe (1H/13C/19F/31P-2H) |
 | Varian
5mm Broad Band Probe (1H-X-2H) |
 | Varian
10mm Broad Band Probe (1H-X-2H) |
 | Nalorac 20 mm Broad
Band Probe (1H-X-2H) |
 | Standard
Acquisition, 1H-1H COSY, 1H-13C
DEPT, 1H-13C HETCOR, Relaxation Studies, Multinuclear
(27Al, 17O, 11B, 19F, 31P,
23Na, 2H, 29Si etc) |
Solid
or Liquid-State NMR Experiments Varian
UnityPlus-200 Spectrometer
 | Doty
Scientific Multinuclear 7mm Supersonic
Magic Angle Spinning Solids Probe
(13C, 27Al, 11B, 19F, 31P,
23Na, 2H, 29Si etc) |
 | Varian
5mm Broad Band Liquids Probe (1H-X-2H) |
 | Single Pulse
Acquisition, Cross Polarization (Variable Amplitude), CP Relaxation Studies,
T1/T2 Relaxation Studies |
Process
NMR Analysis (At-Line, Batch, and On-Line) Foxboro
Process NMR Spectrometers (2)
 | Foxboro 57.8 MHz
High-resolution "C-Type" Process FT-NMR (1H NMR) |
 | Foxboro 58.3 MHz
High-resolution "D-Type" Process FT-NMR with ambient-100oC
Variable Temperature Capability |
Low Field NMR
Analysis - "Relaxometry" (H-Content,
SFC Analysis, Oil in Seeds, Oil in Water, Moisture Analysis)
SpinTrack NMR
Analyzer
 | SpinTrack NMR Low
Resolution NMR - Multinuclear (1H, 19F, 11B,
23Na, 31P, 27Al) 10 mm Probes, 1H
Surface Probes. Standard Methods Performed. |
Gas
Chromatography - Simulated
Distillation
 | Shimadzu GC-2010 - Simulated
Distillation Analyzer |
Gas Chromatography -
Mass Spectrometry
 | HP 5890 A with HP 5970 Mass
Selective Detector |
 | HP 5890 A with FID Detector |
Mid-FTIR-ATR
 | NPS IdentifyIR-HVP - Mid-Infrared
Spectroscopy on Solid or Liquid Samples |
For
more information on this topic please contact:
John
Edwards
Manager,
Process and Analytical NMR Services
Process
NMR Associates LLC,
87A
Sand Pit Rd
Danbury,
CT 06810, USA
Tel:
(203) 744-5905
|