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Contact:

John Edwards

(203) 744-5905

Process NMR Associates - Price Schedule         PDF Version          

Rates Standard Rates are Charged for Spectrometer Time and Professional Time

We will Competitively Discount any Quote Obtained from a Commercial NMR Service !!!

Typical Turnaround Time: 1-3 Days from Receipt of Samples. Same Day Priority Turnaround Available on Demand *      

 
NMR Spectrometer Time - 1 Hour Minimum (includes spectrometer set up and routine sample prep).
Standard Rate : $80/hr (For First 4 hours), $35/hr for additional hours over 4 hours (Overnight $500, 24 Hour Acquisitions $800).
Priority Service*: $160/hr for immediate priority. Charge based directly on time to prepare samples, perform analysis and report.
Process FT-NMR and Time-Domain Relaxometer Investigations: $80/hr
Time-Domain NMR Tests - Charged on a per test basis - call for quote.
Professional Time for Interpretation and Non-Standard NMR Related Services: $175 /hr.

* Subject to availability - please inquire

NMR - Individual Experiments:
Standard 1H Analysis : $45 each**  (1 hour minimum, no analysis/interpretation of data/assuming sample not limited (>10 mg))
Standard 13C Analysis : $240** (No analysis/interpretation of data/assuming sample is not limited (>500 mg))
Detailed 13C Analysis with average molecule parameters calculated: $350**
Standard 1H-13C DEPT : $80**  (No analysis/interpretation of data)
Multidimensional experiments will be charged for actual spectrometer time. (Overnight Acquisitions - $500, 24 Hour Acquisitions $800).
Multinuclear and sample-limited experiments will be performed for a length of time that is agreed upon in advance.

** Includes NMR Tube and Standard Deuterated Solvents  !! See Additional Charges that May be Levied Depending on Project Listed Below

Consulting and Interpretation Fees:

Consulting fees are charged at a rate of $175/hr or $1200/day, plus usual/customary expenses.
(Initial discussions concerning a potential project are not considered consulting time).
Expert Witness $350/hr.
Professional Time Associated with NMR Technical Support of Litigation $250/hr

Low Resolution (TD) NMR Service:

T2, CPMG, Inverse Laplace Transformations, T2 Distributions, T1, T1 Distributions - $60 per sample
Temperature Profiles - $150 Per Sample

Simulated Distillation:

D2887 - Boiling Range Distribution of Petroleum Fractions by Gas Chromatography  -  $200 per Sample
D3710 - Boiling Range Distribution of Gasoline and Gasoline Fractions by Gas Chromatography  -  $275 per Sample
D5307 - Boiling Point Distribution of Crude Oil by Gas Chromatography - $275 per Sample
D6352 - Boiling Range Distribution of Petroleum Distillates in Boiling Range from 174 to 700°C by Gas Chromatography - $275 per Sample

Other Analytical Techniques - GC, GC-MS, FT-IR

Call for dedicated quote. 

!! Additional charges:

Non-Standard Solvents - customer will be charged at cost for solvents other than CDCl3, DMSO-D6, or D2O.
Sample Tubes - Customer will be charged at cost for non-standard NMR tubes.
Sample Disposal - Customer will be charged at cost for this service. Typically $5 per sample for disposal. 
Sample Return involves transportation to, and shipment by, a Certified HazMat Shipping Company - cost charged to customer.
Report Mailing  - Customer will be charged at cost for expense of mailing reports by next-day mailing service.
Sample Pick-Up - Samples can be picked up within a 30 mile radius of Danbury at a rate of $40/hr driving time**

 

Process NMR Application Development

Process NMR Acquisition and Chemometric Modeling of Process Stream Sample Sets Available at Rates Negotiated Under an Application Development Agreement (Petrochemical, Refining, Food, Pharmaceutical Applications).

Liquid-State NMR Experiments    Varian Unity-300 Spectrometer

Varian 5mm 4-Nucleus Probe (1H/13C/19F/31P-2H)
Varian 5mm Broad Band Probe (1H-X-2H)
Varian 10mm Broad Band Probe (1H-X-2H)
Nalorac 20 mm Broad Band Probe (1H-X-2H)
Standard Acquisition, 1H-1H COSY, 1H-13C DEPT, 1H-13C HETCOR, Relaxation Studies, Multinuclear (27Al, 17O, 11B, 19F, 31P, 23Na, 2H, 29Si etc)

Solid or Liquid-State NMR Experiments    Varian UnityPlus-200 Spectrometer

Doty Scientific Multinuclear 7mm Supersonic Magic Angle Spinning Solids Probe (13C, 27Al, 11B, 19F, 31P, 23Na, 2H, 29Si etc)
Varian 5mm Broad Band Liquids Probe (1H-X-2H)
Single Pulse Acquisition, Cross Polarization (Variable Amplitude), CP Relaxation Studies, T1/T2 Relaxation Studies

Process NMR Analysis (At-Line, Batch, and On-Line)   Foxboro Process NMR Spectrometers (2)

Foxboro 57.8 MHz High-resolution "C-Type" Process FT-NMR (1H NMR) 
Foxboro 58.3 MHz High-resolution "D-Type" Process FT-NMR with ambient-100oC Variable Temperature Capability

Low Field NMR Analysis - "Relaxometry" (H-Content, SFC Analysis, Oil in Seeds, Oil in Water, Moisture Analysis)  SpinTrack NMR Analyzer

SpinTrack NMR Low Resolution NMR - Multinuclear (1H, 19F, 11B, 23Na, 31P, 27Al) 10 mm Probes, 1H Surface Probes. Standard Methods Performed.

Gas Chromatography - Simulated Distillation 

Shimadzu GC-2010 - Simulated Distillation Analyzer

Gas Chromatography - Mass Spectrometry    

HP 5890 A with HP 5970 Mass Selective Detector
HP 5890 A with FID Detector

Mid-FTIR-ATR 

NPS IdentifyIR-HVP - Mid-Infrared Spectroscopy on Solid or Liquid Samples
 

Sample Submission  - Follow this link for details on how to submit a sample.

 

 

 

For more information on this topic please contact:

John Edwards

Manager, Process and Analytical NMR Services

Process NMR Associates LLC,

87A Sand Pit Rd

Danbury, CT 06810, USA

Tel: (203) 744-5905